Practical Process Engineering

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The four (4) most common methods of batch gas purging are:syphon, vacuum, pressure, and sweep-throughSyphon purging involves filling the vessel with liquid (product or water) and then the gas purge is introduced into the vapor space and the liquid is drained. The purge gas volume is equal to the volume of the vessel.Vacuum purging is perhaps the most common method for purging vessel rated for the needed vacuum condition. Vacuum is drawn on the vessel and then purge gas is used to relieve the vessel to atmospheric pressure. This proceed is often repeated until an acceptable level of a component (usually oxygen) is reached. The acceptable level will determine the number of cycles that will be necessary.Pressure purging involves the introduction of the purge gas under pressure to dilute the component gas. Then the vessel is relieved to atmosphere (or other treatment device depending on the gas component to be diluted). Then additional pressure cycles can be executed to reach the desired component level.Sweep-through purging is common used for vessels that are not rated for sufficient pressure or vacuum conditions. Purge gas enters one connections and is simultaneously withdrawn from another connection until the component level is within acceptable limits.Reference: CEP Magazine, February 2001

Example 2

Example 1

It is not very hard to calculate required nitrogen. First of all you have to choose the purging method and then find the LOC (limiting oxygen concentration) for your process fluid. Calculations are based on ideal gas law. Sometimes, nitrogen stream has some impurities. Make sure you add this to your calculations. Here are some papers and references.

can any one share Nitrogen Purging calculations sheet?

Whenever the system gas pressure or vacuum exceeds the setting, the pallet is designed to lift. Only excess pressure is vented to the atmosphere. Air is drawn into the tank only to relieve an excess vacuum condition. The valve remains closed when the gas utilization system remains within normal operating pressure. The flame arrester is designed to stop the propagation of a flame by absorbing and dissipating heat through the surface area of the bank sheets. Heat is absorbed as ignited gas attempts to pass through the small passages within the bank assembly. This action lowers the temperature of the gas below its ignition point and quenches the flame.

Pressure relife/ vacuum valve+ flame arrester (all in one) for low pressure storage tanks

The diaphragm constantly senses the upstream gas pressure. The backpressure valve will remain closed until the line pressure exceeds the set point, maintaining a pre-determined back pressure throughout the system. When the pressure in the line exceeds the set point, the diaphragm will operate to open the valve, allowing flow. When the pressure in the line drops below the set point, the valve returns to the closed position. While gas is flaring, the flame arrester and thermal by pass shut-off valve serve to inhibit a possible flashback of the flame into the gas piping. If a flashback occurs downstream of the assembly, the flame arrester prevents the propagation of flame by dissipating the heat, so that the temperature upstream of the unit remains below the ignition temperature of the gas.Should the flame continue to burn, the fusible element in the thermal bypass shut-off valve will melt. This allows the pressure on the top and bottom of the diaphragm to equalize. The spring will then close the main valve, shutting off the gas supply and quenching the flame.